TC3403 INSTRUMENTAL METHODS OF CHEMICAL ANALYSIS SYLLABUS | ANNA UNIVERSITY B.TECH TEXTILE CHEMISTRY 7TH SEM SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY SEVENTH SEMESTER B.TECH TEXTILE CHEMISTRY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI,TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
TC3403 INSTRUMENTAL METHODS OF CHEMICAL ANALYSIS L T P C
3 0 0 3
UNIT I 9
Visible spectrometry, UV-VIS Spectrophotometry and Colorimetry – Theory, Deviations
from Beer’s Law, Instrumentation (Line diagram alone) and application. Ultra violet
spectroscopy – Theory, instrumentation and application – Quantum description,
Instrumentation, Chemical shift, applications and limitations.
UNIT II 9
Infra red spectroscopy, FTIR, ATR-FTIR – Theory, Fundamental Vibrations, Overtones,
Hook’s Law. Instrumentation, Single and Double beam spectrometers, Application and
Limitations, Difference between Raman spectra and IR spectra. Mass spectroscopy –
Theory, Spectrometers, Interpretation, some examples, applications and limitations, XRay
Photo electron spectroscopy (XPS).
52
UNIT III 9
Conduct metric measurements – Important Laws, Definitions, conductance
measurements, applications, Types, advantages and disadvantages of Conduct metric
titration’s.
Potential measurements, pH determination, Ion selective electrodes, Application of pH
measurements, (pH paper, solution) Type of potentiometer titration’s advantages, pH
Buffers and standardization.
Thermal methods – Thermogravimetry, differential Thermal analysis, Thermometric
titration’s and their applications.
UNIT IV 9
Chromatographic techniques – Introduction and classification. Theory, Instrumentation
and Application of Paper chromatography, Thin Layer Chromatography, Column
Chromatography, Gas Chromatography, High performance liquid Chromatography, Gas-
Liquid Chromatography.
UNIT V 9
Errors, Precision and Accuracy: Definitions, Significant figures, Types of errors, Methods
of expressing accuracy and precision, confidence limits.
TOTAL : 45 PERIODS
REFERENCE BOOKS
1. Bona,M., “Modern control Techniques in textile finishing and making up”, Eurotex,
Blachwells Bookshop, London, 2001
2. Banwell,G.C., “Fundamentals of molecular spectroscopy”, TMH, 2003.
3. Day, R.A., and Unerwood, A.L., “Qualitative inorganic analysis, 5th edition”, Prentice-
Hall of India, New Delhi, 2004.
4. Rouessac,F., “Chemical analysis – modern international method and techniques”,
Wiely, New Delhi, 1999.
TC3403 INSTRUMENTAL METHODS OF CHEMICAL ANALYSIS L T P C
3 0 0 3
UNIT I 9
Visible spectrometry, UV-VIS Spectrophotometry and Colorimetry – Theory, Deviations
from Beer’s Law, Instrumentation (Line diagram alone) and application. Ultra violet
spectroscopy – Theory, instrumentation and application – Quantum description,
Instrumentation, Chemical shift, applications and limitations.
UNIT II 9
Infra red spectroscopy, FTIR, ATR-FTIR – Theory, Fundamental Vibrations, Overtones,
Hook’s Law. Instrumentation, Single and Double beam spectrometers, Application and
Limitations, Difference between Raman spectra and IR spectra. Mass spectroscopy –
Theory, Spectrometers, Interpretation, some examples, applications and limitations, XRay
Photo electron spectroscopy (XPS).
52
UNIT III 9
Conduct metric measurements – Important Laws, Definitions, conductance
measurements, applications, Types, advantages and disadvantages of Conduct metric
titration’s.
Potential measurements, pH determination, Ion selective electrodes, Application of pH
measurements, (pH paper, solution) Type of potentiometer titration’s advantages, pH
Buffers and standardization.
Thermal methods – Thermogravimetry, differential Thermal analysis, Thermometric
titration’s and their applications.
UNIT IV 9
Chromatographic techniques – Introduction and classification. Theory, Instrumentation
and Application of Paper chromatography, Thin Layer Chromatography, Column
Chromatography, Gas Chromatography, High performance liquid Chromatography, Gas-
Liquid Chromatography.
UNIT V 9
Errors, Precision and Accuracy: Definitions, Significant figures, Types of errors, Methods
of expressing accuracy and precision, confidence limits.
TOTAL : 45 PERIODS
REFERENCE BOOKS
1. Bona,M., “Modern control Techniques in textile finishing and making up”, Eurotex,
Blachwells Bookshop, London, 2001
2. Banwell,G.C., “Fundamentals of molecular spectroscopy”, TMH, 2003.
3. Day, R.A., and Unerwood, A.L., “Qualitative inorganic analysis, 5th edition”, Prentice-
Hall of India, New Delhi, 2004.
4. Rouessac,F., “Chemical analysis – modern international method and techniques”,
Wiely, New Delhi, 1999.
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