PL9316 POLYMER SCIENCE LAB SYLLABUS | ANNA UNIVERSITY MTECH POLYMER TECHNOLOGY 1ST SEM SYLLABUS REGULATION 2009 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FIRST SEMESTER M.TECH POLYMER TECHNOLOGY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2009 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PL9316 POLYMER SCIENCE LABORATORY L T P C
0 0 4 2
16
1. Polymer synthesis – bulk, solution, emulsion, suspension and slurry polymerisations -
low and high temperature condensation polymerisation, interfacial polycondensation,
thermal and redox initiated polymerisations.
2. Kinetics of polymerisation – dilatometry, gravimetry. 10
14
3. Determination of reactivity ratio of MMA – styrene copolymer – characterisation by TGA,
TMA, NMR and IR. Crystallinity of polymers – X-ray diffraction study.
10
4. Molecular weight determination – viscometry, end group analysis, GPC, light scattering,
osmometry.
10
5. Fractionation of polymers – Fractional precipitation method – polydispersity
TOTAL: 60 PERIODS
REFERENCES
1. Edward A. Colloind, J.Bares and F.W. Billmeyer Jr., Experiments in Polymer Science,
Wiley Interscience, New York 1973.
2. Wayne R.Sorenson and T.W.Campbell, Preparative Methods of Polymer Chemistry 3nd
edition, Wiley – Interscience, New York, 2001.
3. E.M.McCaffery, Laboratory Preparation for Macromolecular Chemistry, McGraw Hill,
Kogakush 1970.
PL9316 POLYMER SCIENCE LABORATORY L T P C
0 0 4 2
16
1. Polymer synthesis – bulk, solution, emulsion, suspension and slurry polymerisations -
low and high temperature condensation polymerisation, interfacial polycondensation,
thermal and redox initiated polymerisations.
2. Kinetics of polymerisation – dilatometry, gravimetry. 10
14
3. Determination of reactivity ratio of MMA – styrene copolymer – characterisation by TGA,
TMA, NMR and IR. Crystallinity of polymers – X-ray diffraction study.
10
4. Molecular weight determination – viscometry, end group analysis, GPC, light scattering,
osmometry.
10
5. Fractionation of polymers – Fractional precipitation method – polydispersity
TOTAL: 60 PERIODS
REFERENCES
1. Edward A. Colloind, J.Bares and F.W. Billmeyer Jr., Experiments in Polymer Science,
Wiley Interscience, New York 1973.
2. Wayne R.Sorenson and T.W.Campbell, Preparative Methods of Polymer Chemistry 3nd
edition, Wiley – Interscience, New York, 2001.
3. E.M.McCaffery, Laboratory Preparation for Macromolecular Chemistry, McGraw Hill,
Kogakush 1970.
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